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MFT低成膜溫度測(cè)定儀

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一、產(chǎn)品簡(jiǎn)介 

I. brief introduction

聚合物乳液用作涂料、粘合劑、化纖織物、皮革、紙張等表面的處理劑時(shí),它的成膜性是重要的技術(shù)指標(biāo)之一。研究者為了制造出更低成膜溫度的新產(chǎn)品來,不斷地改進(jìn)其技術(shù)規(guī)范和配方。因此檢測(cè)出低成膜溫度(MFT)是此類涂料的重要指標(biāo),能夠方便的測(cè)出MFT的理想儀器。MFT型低成膜溫度測(cè)定儀是依據(jù)國(guó)家標(biāo)準(zhǔn)GB9267-2008而設(shè)計(jì)制造的,它是新一代漆膜測(cè)試儀,具有國(guó)內(nèi)外傳統(tǒng)測(cè)試儀器的諸多優(yōu)點(diǎn),又融合了臺(tái)式、節(jié)能、超寬工作臺(tái)、測(cè)溫準(zhǔn)確等優(yōu)點(diǎn)于一體,成為同類儀器之佼佼者。本手冊(cè)中的所有圖片和產(chǎn)品規(guī)格參數(shù)僅供參考,實(shí)際產(chǎn)品可能會(huì)略有差異,恕不另行通知。

When polymer emulsion is used as coating, binder, chemical fiber, fabric, leather, paper and other surface treatment agent, its film forming property is one of the important technical indexes. The researchers continually improved their technical specifications and formulations in order to produce new products with lower film forming temperatures. Therefore, the detection of the minimum film forming temperature (MFT) is an important indicator of this kind of coating, and it can conveniently measure the ideal instrument of MFT. MFT minimum film-forming temperature measurement instrument is designed and manufactured according to the national standard GB9267-2008, it is a new generation of film tester has many advantages at home and abroad test instrument, and the integration of the desktop, energy saving, wide working platform, accurate temperature measurement method, as a leader in similar instruments. All the pictures and product specifications in this manual are for reference only, and the actual products may be slightly different without notice.

二、主要參數(shù)

Two, the main parameters

★梯度板工作溫度范圍:冷端低 -7℃熱端高 70℃

This gradient in the temperature range: -7 DEG end at the cold end heat up to 70 DEG C

★梯度板檢測(cè)點(diǎn):13 個(gè)

Detection point: 13. Gradient plate

★梯度間隔:20mm

Gradient interval: 20mm.

★試驗(yàn)涂料槽:6 條 , 長(zhǎng)度 240mm,寬度 22mm 深度 0.25mm

This test: 6 coating groove length 240mm, width 22mm, depth 0.25mm

★巡檢表顯示:16 點(diǎn),其中 1 ~ 13 點(diǎn)為工作梯度溫度,14 點(diǎn)為儀器環(huán)境溫度,15、16 點(diǎn)為冷卻水進(jìn)出口溫度

This inspection table shows: 16 points, including 1 to 13 points for 14 points for the instrument temperature gradient, ambient temperature, 15, and 16 points for the cooling water inlet temperature

★電源:220v 50Hz 交流寬電壓(三相電源,接地良好)

* power supply: 220V 50Hz AC voltage (three-phase power supply, good grounding)

★冷卻水源:普通市政供水

Cooling water: ordinary municipal water supply.

★儀器外形 : 尺寸長(zhǎng) 520mm× 寬 520mm× 高 370mm(大部分)

*: instrument appearance size length 520mm width 520mm and height 370mm (the largest part)

★儀器重量 :31Kg

Instrument weight: 31Kg.

三、儀器特點(diǎn)

Three, instrument characteristics

★臺(tái)式機(jī)設(shè)計(jì),更節(jié)省空間。

Design * desktop, save more space.

★更先進(jìn)的梯度板設(shè)計(jì),以便更大的縮減體積。

Gradient plate design more advanced. In order to further reduce the size.

★表面溫度校準(zhǔn),配合溫度標(biāo)尺,確保測(cè)定數(shù)據(jù)準(zhǔn)確可靠。

* the surface temperature with the temperature scale, accurate calibration, ensure the data accurate and reliable determination.

★自動(dòng)斷水保護(hù)系統(tǒng)。

Automatic water cut-off protection system.

★更寬的工作臺(tái),可以同時(shí)測(cè)量 6 組樣品。

Table. The wider, 6 groups of samples can be measured at the same time.

四、使用方法

Four, the use of methods

打開包裝箱,(包裝箱可以反復(fù)利用,請(qǐng)妥善保管,以便以后維修運(yùn)輸之用)檢查一下有無破損短缺現(xiàn)象。核實(shí)后,將儀器安放在試驗(yàn)室靠近上下水之處,先做一下清潔工作。然后查看電源輸入,進(jìn)出水口接牢無誤。

Open the packing box (the packing box can be used again and again, please keep it for future maintenance and transportation). Check for any breakage. After verification, put the instrument in the laboratory, near the upper and lower parts of the water, do some cleaning work first. Then check the power input and make sure the inlet and outlet are secure.

使用前的準(zhǔn)備工作:

Preparation prior to use:

★開機(jī):

Boot:

將電源線接入電源插座(220 伏,50Hz 三孔插座,接地良好),接通冷卻水,依次接通總電源開關(guān)、加熱、巡檢、制冷開關(guān),儀器面板立即顯示出相應(yīng)動(dòng)作(指示燈亮,數(shù)顯表顯示數(shù)字)。

The power line access power socket (220 V, 50Hz socket, must be well grounded), connected to the cooling water, turn on the power switch, heating, cooling, inspection switch, instrument panel immediately show the corresponding action (indicator lights, digital display digital).

★調(diào)試儀表:

By debugging instrument:

根據(jù)所測(cè)試漆膜條件不同,需設(shè)置不同測(cè)試條件。主要是制冷和加熱預(yù)置(設(shè)置方法見 LU-906M 智能調(diào)節(jié)器使用說明書),巡檢表在出廠前已調(diào)好,一般情況下不需調(diào)整。

Different test conditions need to be set according to different test conditions. Mainly refrigeration and heating preset (set method see LU-906M intelligent controller manual), the inspection table before the factory has been adjusted, in general, need not adjust.

★熱平衡:

By the heat balance:

時(shí)間約在 120 分鐘左右(視設(shè)定溫度而定,若發(fā)現(xiàn)巡檢表在時(shí)間內(nèi) 1 ~ 13 各點(diǎn)顯示穩(wěn)定或變化極小即為預(yù)熱完成)方可加入試樣。平衡時(shí)間取決于低溫度設(shè)定,溫度設(shè)定越低,平衡時(shí)間則越長(zhǎng)。干燥劑同時(shí)放入盒中,可以大限度避免水蒸氣以及冷端結(jié)冰。

Time is about 120 minutes (depending on the setting temperature, if the inspection table is found within a certain period of time, 1~13 points show stability or minimal change, that is, preheating is completed), you can join the sample. The balance time depends on the minimum temperature setting, and the lower the temperature setting, the longer the equilibrium time. The desiccant is also placed in a box to minimize water vapor and cold end ice.

五、樣品準(zhǔn)備

Five sample preparation

取下玻璃罩用小勺或滴管將待測(cè)和已知乳液注入梯度板槽內(nèi),再用涂布器涂平,蓋好玻璃罩。(玻璃制品,請(qǐng)輕拿輕放)

Remove the glass cover, use a spoon or dropper to inject the tested and known emulsion into the gradient plate trough, then coat it with a coater and cover the glass cover. (glass, please handle with care.)

★樣品成膜:

The film samples:

大約經(jīng)過 60 ~ 90 分鐘,梯度板上的涂層發(fā)生一系列的變化,乳膠漆用乳液水分蒸發(fā)后,聚合物分子相互作用,在適當(dāng)溫度下形成連續(xù)薄膜,高于該乳液 MFT 的部分成膜透明,低于 MFT 的部分發(fā)生龜裂或產(chǎn)生白堊現(xiàn)象。這個(gè)明顯的分界線即為該乳液的低成膜溫度(MFT)確定成膜線后,根據(jù)其位置,用標(biāo)尺的細(xì)分刻度計(jì)算出準(zhǔn)確溫度。

After about 60 to 90 minutes, the coating plate on the gradient of a series of changes, the latex emulsion evaporation, interaction between polymer molecules, forming a continuous film at a suitable temperature is higher than that of the MFT part of the emulsion film is transparent, less than MFT part of the crack or produce chalk phenomenon. The obvious dividing line is the minimum film forming temperature (MFT) of the emulsion. After determining the film forming line, the accurate temperature is calculated by the scale of the ruler according to its position.

★關(guān)機(jī):

* shutdown:

試驗(yàn)完畢后,關(guān)閉電源、水源,做好各部位的清潔工作,為下一次試驗(yàn)做好準(zhǔn)備。

After the test, turn off the power, water, do a good job cleaning the parts, prepare for the next test.

六、注意事項(xiàng)及使用技巧

Six, attention and use skills

★儀器放置在通風(fēng)明亮的實(shí)驗(yàn)室內(nèi),勿受潮濕。儀器不用時(shí)須罩上塑料罩,保持干凈。

This instrument is placed in ventilated and bright laboratory, keep dry. The instrument should be covered with plastic when not in use. Keep it clean.

★電源要求:220 伏,50Hz,> 400W,三孔插座,接地良好。

* power requirements: 220 V, 50Hz, 400W, socket, good grounding.

★環(huán)境要求:溫度 23±2℃,相對(duì)濕度<85%,無陽(yáng)光直射,無振動(dòng)的環(huán)境。

* environmental requirements: temperature 23 - 2 DEG C, relative humidity<85%, no sunlight, no vibration environment.

★水源要求:無雜質(zhì),純凈自來水,須保持流暢。

* water requirements: no impurities, clean tap water, to maintain smooth.

★測(cè)試條件主要是制冷和加熱的設(shè)定。制冷主要影響低溫端工作,以第一點(diǎn)要求為準(zhǔn)。加熱主要影響高溫端工作,以第十三點(diǎn)要求為準(zhǔn)。盡量減小冷熱差,即節(jié)能,又可提高分辨率,

It is the main test conditions of heating and refrigerating set. The refrigeration mainly affects the low temperature end, and the first point is required. Heating mainly affects high temperature end work, whichever is required by thirteenth points. Minimize cold and heat difference, that is, energy saving, but also to improve the resolution,

★工作臺(tái)使用前后要清洗,長(zhǎng)時(shí)間放置時(shí)涂些油脂或凡士林,以防銹蝕。

This table should be cleaned before and after use, place a long time when coated with grease or vaseline to prevent rust.

★涂布待測(cè)乳液時(shí),至少要有一條已知材料,以作對(duì)照之用。

* to be measured when the emulsion coating, must have at least one known material for control purposes.

★涂布乳液時(shí)不要涂滿測(cè)試槽,只要涂在估計(jì)MFT 左右即可,既省工料又好清洗。

You don't have to emulsion coating painted test tank, as long as the painted around MFT can be estimated, both quantity and good cleaning.

★用衛(wèi)生紙條放置在梯度板左右邊緣,以防涂布和清洗時(shí)弄臟工作臺(tái)。

I use note placed at the edge of the gradient in health, to prevent the coating and cleaning dirty work station.

★為了清洗方便,板表面可以覆蓋一層薄的鋁箔(如0.02mm 厚), 用刷子將其刷平 , 可滴幾滴甘油使鋁箔和板面緊密結(jié)合。

In order to more convenient cleaning, the plate surface can be covered with a layer of thin aluminum foil (0.02mm thick), use the brush to brush the flat, a few drops of glycerin and combination of aluminum foil surface.

★干燥劑選用氯化鈣 (CaCl2 ) 效果更佳。

I used calcium chloride desiccant (CaCl2) effect is better.

七、裝箱清單

Seven packing list

★主機(jī) 1 臺(tái)

The 1 computers.

★玻璃罩 1 個(gè)

The glass cover 1.

★干燥劑盒 2 個(gè)

The desiccant box 2.

★干燥劑 1 罐

* 1 cans of desiccant

★電源線 1 根

Power line 1.

★水導(dǎo)管 2 根(用于上水和下

2. Water conduit (for under water and root



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